Microdiffusion Analysis and Volumetric Error

PART I – APPARATUS AND PRINCIPLES USED IN MICRODIFFUSION ANALYSIS – II. A STANDARD MICRO DIFFUSION APPARATUS OR ‘UNIT’ – III. FACTORS INFLUENCING THE ABSORPTION RATE FROM OUTER TO INNER CHAMBER WITH SPECIAL REFERENCE TO AMMONIA – IV. GENERAL PRINCIPLES GOVERNING THE ABSORPTION TIME IN MICRO DIFFUSION ANALYSIS – V. PIPETTES (SUITABLE FOR USE WITH THE STANDARD UNITS) AND THEIR DELIVERY ERRORS – VI. MICRO-BURETTES (SUITABLE FOR USE WITH THE STANDARD UNITS) AND ERRORS INVOLVED IN THEIR USE – VII. THE MICRODIFFUSION METHOD WITH END-POINT VOLUMES AROUND 20 CUBIC MILLIMETRES – VII. COLORIMETRY IN THE MICRODIFFUSION METHODS – PART II – DESCRIPTION OF METHODS WITH THE STANDARD UNITS – IX. AMMONIA. GENERAL METHOD USING STANDARD ACID AS ABSORBENT – X. AMMONIA. GENERAL METHOD (USING THE BORIC-HCL PROCEDURE) – XI. SPECIAL FACTORS INFLUENCING THE RATE OF AMMONIA ABSORPTION – XII. OTHER METHODS FOR DETERMINING THE ABSORBED AMMONIA IN THE MICRO DIFFUSION PROCEDURE – XIII. AMMONIA. BIOLOGICAL DETERMINATIONS – XIV. TOTAL NITROGEN XVII. UREA (BLOOD AND URINE) – XIX. ADENOSINETRIPHOSPHORIC ACID, ADENYLIC ACID, ADENOSINE, ETC. – XX. NITRATE, NITRITE AND AMIDE NITROGEN – XXII.
MONOAMINE OXIDASE AND HISTAMINASE IN TISSUES – XXIII. DETERMINATION OF VOLATILE AMINES – XXIV. CARBONATES AND BICARBONATE – XXV. BLOOD GLUCOSE AND FERMENTABLE SUGAR IN NORMAL URINE – XXVI. DETERMINATION OF CARBONIC ANHYDRASE – XXVII. OXIDATION RATES OF ORGANIC SUBSTANCES WITH A STANDARD OXIDANT WITH APPLICATION TO DETERMINATION OF MINUTE AMOUNTS OF CALCIUM AS OXALATE – XXVIII. ACETIC ACID AND OTHER LOWER FATTY ACIDS – XXIX. ASSAY OF ACETYLCHOLINESTERASE – XXX. CYANIDE, AZIDE, SULPHIDE, PHENOLS – XXXI. METHANOL AND ISOPROPANOL GROUP – XXXII. ETHANOL – XXXIII. ETHANOL FROM URETHANE – XXXIV. FORMALDEHYDE – XXXV. FORMALDEHYDOGENIC STEROIDS (PERIODIC ACID AS OXIDANT) – XXXVI. FORMALDEHYDOGENIC STEROIDS (SODIUM BISMUTHATE AS OXIDANT) – XXXVII. GLYCINE (FORMALDEHYDE PRODUCED BY NINHYDRIN OXIDATION) – XXXVIII. ACETALDEHYDE (SEMICARBAZIDE ABSORPTION) – XXXIX. ACETALDEHYDE FROM LACTIC ACID AND THREONINE WITH BISULPHITE ABSORPTION – XL. ACETONE (INCLUDING A RAPID CLINICAL METHOD USING THE NESSLER SOLUTION) – XLI. THE HALOGENS (INTRODUCTORY) – XLII. CHLORIDE (BY OXIDATION TO CHLORINE AND ABSORPTION INTO IODIDE) – XLIII. CHLORIDE (BY OXIDATION TO CHLORINE AND ABSORPTION INTO FAST GREEN) – XLIV.
BROMIDE – XLV. IODIDES AND HALOGEN MIXTURES – XLVI. SERIAL DETERMINATION OF ORGANICALLY BOUND HALOGEN – XLVII. VOLATILE HALOGENATED HYDROCARBONS (CHLOROFORM, TRICHLORETHYLENE AND CARBON TETRACHLORIDE) – XLVIII. CARBON MONOXIDE – XLIX. A RAPID CLINICAL METHOD FOR CARBON MONOXIDE DETERMINATION – LI. TOTAL MOLECULAR CONCENTRATION IN FLUID SAMPLES OF ABOUT 3-4 MILLIGRAMS – LII. SEPARATION OF CRYSTALS AND’ GUMS’ BY MICRODIFFUSION – QUALITATIVE MICRO-DIFFUSION ANALYSIS – LIII. SOME CONSIDERATIONS ON QUALITATIVE MICRO-DIFFUSION ANALYSIS – PART III – THE ERROR OF VOLUMETRIC TITRATION – LIV. INTRODUCTORY – LV. THE VARIABLE GLASS ERROR – LVI. THE TOTAL VARIABLE GLASS ERROR AND ITS CONTROL – LVII. THE VARIABLE CHEMICAL ERROR IN TITRATION – LVIII. THE RATIONALE OF MICRO TITRATION – LIX. THE CONSTANT GLASS ERROR – LX. THE CONSTANT CHEMICAL ERROR – LXI. VOLUMETRIC ERROR IN KJELDAHL NITROGEN ANALYSES – LXIII. UREA EXCRETION AS RENAL FUNCTION TEST – Full TOC available on website